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- W2022602086 abstract "Abstract Aliphatic phenylchloronium ylide with bis(trifluoromethylsulfonyl)‐methylidene group was synthesized. Thermal transylidation of 4‐(trifluoromethyl)phenylbromonium bis(trifluoromethylsulfonyl)methylide in chlorobenzene as a solvent at 130°C afforded phenylchloronium bis(trifluoromethylsulfonyl)methylide in a moderate yield. Phenylbromonium and phenyliodonium ylides were also prepared by the thermal transylidation to bromo‐ and iodobenzenes. The reaction probably involves initial thermal generation of bissulfonylcarbene (Tf 2 C:), followed by nucleophilic attack of a halobenzene toward the electron‐deficient carbene center. Solid‐state structures of these aliphatic phenylhalonium ylides were analyzed and compared with each other. © 2011 Wiley Periodicals, Inc. Heteroatom Chem 22:325–330, 2011; View this article online at wileyonlinelibrary.com . DOI 10.1002/hc.20683" @default.
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- W2022602086 date "2011-01-01" @default.
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- W2022602086 title "Synthesis and structure of aliphatic phenylchloronium ylide" @default.
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