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- W2022609958 abstract "µ-2,2′-Azobispyridinebis[2,2′-azobispyridinesalicylato(O)salicylato(O,O′) cadmium(II)], (µ-abpy)[Cd(Hsal)2(abpy)]2 (I) was synthesized and characterized by IR and UV/ Vis spectroscopy, thermal analysis, and X-ray diffraction techniques. Two abpy ligands and two salicylato ligands coordinate to the Cd2+ ion in a monocapped trigonal-prismatic arrangement. The capping atom is the N3 atom. One of the two abpy ligands behaves as a “s-frame” bridging ligand and adopts a s-cis/ E/ s-cis conformation, whereas the other one adopts as a s-cis/ E/ s-trans conformation. One of the two salicylato ligands acts as a monodentate ligand, which coordinates with the carboxylate oxygen atom, whereas the other one adopts bidentate coordination through two carboxylate oxygen atoms. The hydroxy groups of salicylato ligands, which coordinate in a monodentate fashion, are disordered over two positions, with occupancies of 0.52 for group A and 0.48 for group B. The decomposition reaction takes place in the temperature range 20–1000 °C under nitrogen. Thermal decomposition of the title complex proceeds in two stages." @default.
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- W2022609958 date "2010-05-31" @default.
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- W2022609958 title "Synthesis, Crystal Structures and Spectrothermal Characterization of a Heptacoordinated Dimeric Salicylato Cadmium(II) Complex with 2,2′-Azobispyridine (abpy), (µ-abpy)[Cd(Hsal)2(abpy)]2" @default.
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- W2022609958 doi "https://doi.org/10.1002/zaac.200900333" @default.
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