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- W2022648135 abstract "The structural and chemical evolution of propionate based low fluorine YBa2Cu3O7 − δ (YBCO) precursor during the conversion thermal treatment to obtain superconducting film has been investigated by both x-ray photoelectron and diffraction techniques in a set of partially converted films on SrTiO3 single crystals. The pyrolysis temperature within the range 400–480 °C mainly affects the copper valence state with an increase of the Cu2 + fraction with temperature with respect to the Cu1 + oxidation state. During the subsequent thermal treatment up to 700 °C, the reduction of fluorine content is mainly ascribed to the hydrolysis of YF3. At higher temperatures, Ba hydrolysis, Y2Cu2O5 and YBCO phase formation (nucleation at 700 °C and 725 °C, respectively) have been observed. The temperature dependences of the formation and decomposition of YBCO, Y2Cu2O5 and Ba-oxyfluoride were evaluated by x-ray diffraction measurements. The reaction path emerging from these analyses agrees with the one observed for YBCO films obtained with the standard MOD method based on metal tri-fluoroacetate precursors." @default.
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- W2022648135 date "2011-10-07" @default.
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- W2022648135 title "Structural and chemical evolution of propionate based metal–organic precursors for superconducting YBa<sub>2</sub>Cu<sub>3</sub>O<sub>7 − δ</sub>epitaxial film growth" @default.
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- W2022648135 doi "https://doi.org/10.1088/0953-2048/24/11/115008" @default.
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