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• W2022671401 abstract "AbstractRutile solid solutions Crx Ti1-2xTaxO2 (0 < x < 0·5) have been synthesised by: firing mixtures of Cr2O3 , Ta2O5 , and TiO2 (anatase); firing colloidal gels obtained from TiCl4 , TaCl5 , and CrCl3 . 6H2O; and firing polymeric gels prepared from Ti4+ isopropoxide, Ta5+ethoxide, and Cr3+ acetylacetonate at 300–1300°C. Samples were characterised by XRD, differential thermal and thermogravimetric analysis, UV visible spectroscopy, Cielab colour parameter measurements, and electron microscopy. In samples synthesised from oxide mixtures, CrTaO4 (rutile structure) appeared as an intermediate phase in the formation of the solid solutions and a positive departure from Vegard's law was observed. Ta2O5 segregation in gel samples seems to prevent the formation of material consisting only of rutile. The distortion of MO6 octahedra varies as x increases. The chemical, structural, and thermal stability, and the colouration obtained on glazes containing 3 wt-%samples, indicate their potential for use as ceramic pigments. Under the experimental conditions used, the materials prepared by sol–gel synthesis were not found to be better than those prepared from oxide mixtures." @default.
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• W2022671401 date "2000-05-01" @default.
• W2022671401 modified "2023-09-27" @default.
• W2022671401 title "Influence of precursors on formation of TiO₂–CrTaO₄rutile solid solutions" @default.
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• W2022671401 doi "https://doi.org/10.1179/096797800680983" @default.
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