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- W2022690645 abstract "Die Enthalogenierung von Isopropyldichlorphosphan und sec-Butyldichlorphosphan mit Magnesium führt zu den Titelverbindungen (i-PrP)3 (1) bzw. (s-BuP)3 (2). Als Nebenprodukte werden die entsprechenden Cyclotetraphosphane, im Fall von 1 auch noch (i-PrP)5, gebildet. 1 und 2 sind relativ beständige Triorganyl-cyclotriphosphane, die in reiner Form isoliert und vollständig charakterisiert werden konnten. Auf Grund der chiralen P-gebundenen Kohlenstoffatome bildet 2 vier 31P-NMR-spektroskopisch unterscheidbare Konfigurationsisomere. Contributions to the Chemistry of Phosphorus. 119. Tri-isopropyl-cyclotriphosphane, (i-PrP)3, and Tri-sec-butyl-cyclotriphosphane, (s-BuP)3 The dehalogenation of isopropyldichlorophosphane and sec-butyldichlorophosphane with magnesium leads to the title compounds (i-PrP)3 (1) and (s-BuP)3 (2) respectively. The corresponding cyclotetraphosphanes, and in the case of 1 also (i-PrP)5, are formed as by-products. 1 and 2 are relatively stable triorganyl-cyclotriphosphanes. They were isolated in a pure state and have been fully characterized. Due to the chiral P-bonded carbon atoms 2 forms four diastereomers, which could be identified by NMR spectroscopy." @default.
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- W2022690645 date "1983-03-01" @default.
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- W2022690645 title "Beitr�ge zur Chemie des Phosphors. 119. Tri-isopropyl-cyclotriphosphan, (i-PrP)3, und Tri-sec-butyl-cyclotriphosphan, (s-BuP)3" @default.
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