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- W2022707621 abstract "Starting from cholesterol the three possible stereoisomeric 1,4-benzodioxanes 24, 31, 32 and a series of analogues with 2βH,3βH configuration (25–27, 29, 30) have been synthesized. The α band of the 1,4-benzodioxane chrompohore has been unequivocally identified in the CD spectra between 325–300 nm. For its Cotton effect the same helicity rule is valid as for homochirally analogous tetralins: the P/M helicity of the heteroring leads to a positive/negative CD within the α-band. The (2′R,3′R) configuration of 6 has been established by a comparison of its CD data with those of 39 and with the help of the above-mentioned helicity rule. This allows the assignement of the (2S,2′R,3′R) configuration of (−)-silandrin (3)." @default.
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- W2022707621 date "1991-07-12" @default.
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- W2022707621 title "Synthesis and circular dichroism of steroids with a 1,4-benzodioxane chromophore: On the absolute configuration of (−)-silandrin" @default.
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- W2022707621 doi "https://doi.org/10.1002/jlac.1991199101115" @default.
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