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- W2022760039 endingPage "6107" @default.
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- W2022760039 abstract "Zn-mediated allylation and propargylation of (R)-2,3-O-cyclohexylideneglyceraldehyde (1) in aqueous medium following Luche's procedure afforded the anti homoallylic 3 and homopropargylic 8 alcohols in good yield and with high stereoselectivity. Crotylation of 1 under similar conditions afforded appreciable amounts of erythro-5 and threo-6 alcohols. In each case, the diastereo alcohols are separable by column chromatography. Compound 8 on appropriate chemical manipulation of its functionalities gave the (S)-enantiomer of (R)-13, a useful synthon of LTB(4). Compound 3 on chemical elaboration afforded a diversely functionalized triol derivative 15, a potentially useful synthon for many bioactive compounds." @default.
- W2022760039 created "2016-06-24" @default.
- W2022760039 creator A5070042579 @default.
- W2022760039 date "1996-01-01" @default.
- W2022760039 modified "2023-10-04" @default.
- W2022760039 title "(<i>R</i>)-2,3-<i>O</i>-Cyclohexylideneglyceraldehyde, a Versatile Intermediate for Asymmetric Synthesis of Homoallyl and Homopropargyl Alcohols in Aqueous Medium" @default.
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- W2022760039 doi "https://doi.org/10.1021/jo9604696" @default.
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