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- W2022760103 abstract "We have studied the hydrated and anhydrous dioxynitrate of lead. Pb(NO3)2·2PbO·1.5H2O is obtained by precipitation at 0°C from a 0.75 M lead nitrate solution with concentrated ammonia at a rate of 1.5 ml min−1. By heating between 150 and 300°C the hydrated dioxynitrate gives Pb(NO3)2·2PbO. The progressive calcination of this compound gives PbO with intermediate formation of Pb(NO3)2·5PbO. The hydrated and anhydrous lead dioxynitrate samples were studied by chemical analysis, thermogravimetry, differential thermal analysis, infrared spectroscopy and X-ray powder diffraction. Both dioxynitrates have a laminar structure." @default.
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- W2022760103 date "1986-09-01" @default.
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- W2022760103 title "Obtention, thermal behaviour and structural study of the dioxynitrates of lead" @default.
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