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• W2022778853 abstract "We report a XAFS study of the Fe 3+ local environment in Fe-silicalite as a function of the template burning temperature. We investigate the structural changes of the zeolitic structure, upon thermal treatments and interaction with NH 3 . Our XAFS results show that, before template burring, Fe 3+ are in tetrahedral symmetry with 4 oxygens at 1.85 A, while after template removal and in vacuum conditions, they exhibit a distorted tetrahedral symmetry with 3 oxygens at 1.87 A, and one at 2.10 A; dosage of NH 3 partially restore the tetrahedral symmetry of the site. These results are strongly supported by parallel IR, Raman, UV-Vis, TPR and EPR investigations and by recent theoretical simulations." @default.
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• W2022778853 date "1997-04-01" @default.
• W2022778853 modified "2023-09-27" @default.
• W2022778853 title "Evolution of Fe3+from Framework to Extra-Framework Species in Fe-Silicate as a Function of the Template Burning Temperature" @default.
• W2022778853 doi "https://doi.org/10.1051/jp4:1997275" @default.
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