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- W2022779156 abstract "Vapor phase trap spiking methods have been developed and used for the analysis of volatile organic compounds. Because of their lower vapor pressures, this approach is not suitable for some semivolatile analytes, such as tributyl phosphate (TBP) and dibutyl butyl phosphonate (DBBP). A method was developed to independently quantify TBP and DBBP using a unique trap loading technique, and subsequent thermal desorption/gas chromatographic analysis. Modification of a gas chromatograph injection port allowed methanolic standards to be loaded onto sorbent traps quantitatively. The loaded calibration traps were then thermally desorbed and analyzed. Linearity, reproducibility, accuracy and method detection limits were established and will be reported for TBP and DBBP standards." @default.
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- W2022779156 date "1998-01-01" @default.
- W2022779156 modified "2023-09-27" @default.
- W2022779156 title "Novel calibration technique for headspace analysis of semivolatile compounds" @default.
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- W2022779156 doi "https://doi.org/10.1016/s0021-9673(97)00925-4" @default.
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