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• W2022797769 endingPage "2754" @default.
• W2022797769 startingPage "2745" @default.
• W2022797769 abstract "The complex(es) resulting from a 1:4 mixture of Pd2(DBA)3 and P(o-tol)3 react with aryl bromides or aryl iodides p-XC6H4R (X = Br, I; R = Me, t-Bu, OMe) to generate the corresponding halide dimers {Pd[P(o-tol)3](p-C6H4R)(μ-X)}2 (X = Br, R = t-Bu (1), Me (2), OMe (3); X = I, R = t-Bu (4), Me (5), OMe (6)) in 46−76% yield. Iodide dimer 5 reacts with AgOTf in acetonitrile to form the cationic bis(acetonitrile) complex {Pd[P(o-tol)3](p-C6H4Me)(CH3CN)2]}+OTf- (8) which was treated in situ with LiCl to form the chloride dimer {Pd[P(o-tol)3](p-C6H4Me)(μ-Cl)}2 (9) in 93% yield. The p-tolyl halide dimers 2, 5, and 9 react with N-benzylmethylamine to generate the corresponding 1:1 palladium amine adducts Pd[P(o-tol)3](p-C6H4Me)[HN(Me)Bn]X (X = Cl (12), 85%; X = Br (13), 72%; X = I (14), 77%). Reaction of a mixture of Pd2(DBA)3 and P(o-tol)3 with the haloamines 2-IC6H4(CH2)2N(H)Bn, 2-BrC6H4CH2N(H)(p-tolyl), and 2-BrC6H4(CH2)3N(H)Bn gave the chelated palladium amine complexes Pd[P(o-tol)3](2-C6H4(CH2)2N(H)Bn]I (18, 7..." @default.
• W2022797769 created "2016-06-24" @default.
• W2022797769 creator A5039233288 @default.
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• W2022797769 date "1996-06-11" @default.
• W2022797769 modified "2023-10-10" @default.
• W2022797769 title "Synthesis and Solution Structure of Palladium Tris(<i>o</i>-tolyl)phosphine Mono(amine) Complexes" @default.
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• W2022797769 doi "https://doi.org/10.1021/om9509599" @default.
• W2022797769 hasPublicationYear "1996" @default.
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