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- W2022798812 abstract "Abstract (NMe 4 ) 3 [Fe(NCS) 6 ] crystallizes from ethanol in the monoclinic space group C 2/ c . Two different types of complex ions are contained in the unit cell, though both possess exclusively N ‐coordination of the thiocyanate ligands. In one ion, the thiocyanate ligands are all essentially linearly bound, with an Fe–N–C angle of 174 ± 4°, while in the other, there are two cis ‐thiocyanate ligands with a notably small Fe–N–C angle of 146.5°. The EPR and Mössbauer results show that all the iron( III ) centers maintain the high‐spin state down to 80 K, while the magnetic susceptibility confirms this to 2 K. Infrared and Mössbauer spectra provide evidence for an unusually “soft” lattice. Traditional criteria for interpretation of the infrared frequencies are not strictly applicable for this compound. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005)" @default.
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- W2022798812 date "2005-06-01" @default.
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- W2022798812 title "The Hexakis(thiocyanato)ferrate(<scp>III</scp>) Ion: a Coordination Chemistry Classic Reveals an Interesting Geometry Pattern for the Thiocyanate Ligands" @default.
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- W2022798812 doi "https://doi.org/10.1002/ejic.200400867" @default.
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