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• W2022874481 abstract "Abstract Mg 2+ stabilized Na-β″/β-Al 2 O 3 powder was successfully synthesized by a sol–gel method using PVP-10000 as complexing agent and metal nitrates as corresponding metal sources. The thermal decomposition of the xerogel and the evolution of crystallization behavior of Na-β″/β-Al 2 O 3 were studied. The obtained powders have been unambiguously characterized using X-ray diffraction (XRD), N 2 adsorption, transmission electron microscopy (TEM), and scanning electron microscopy (SEM). The Mg 2+ stabilized Na-β″/β-Al 2 O 3 crystallized gradually from amorphous phase to metastable intermediate phases and further formed the major phase at 1000 °C. The results showed that the large surface area of the amorphous intermediate phase with mesoporous structure followed by the generation of intermediate phases named as m-Al 2 O 3 and MgAl 2 O 4 with spinel structure to a great extent promoted the formation of Na-β″/β-Al 2 O 3 phase. The Na-β″/β-Al 2 O 3 nano-powders exhibited a plate-like two dimensional structure with clear crystallographic plane for Na + diffusion. The transformation from m-Al 2 O 3 only required the shift of Na + from alternate layers of oxygen and the accommodation of every fifth layer since the structure of m-Al 2 O 3 is only slightly different from that of Na-β″/β-Al 2 O 3 . The relative density of the sintered ceramic was approximately 98.8% and the ionic conductivity can reach 0.24 S cm − 1 at 350 °C." @default.
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• W2022874481 date "2014-11-01" @default.
• W2022874481 modified "2023-10-01" @default.
• W2022874481 title "Sol–gel synthesis of Mg2+ stabilized Na-β″/β-Al2O3 solid electrolyte for sodium anode battery" @default.
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• W2022874481 doi "https://doi.org/10.1016/j.jallcom.2014.05.073" @default.
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