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• W2022883235 abstract "Poly(l-lactide) (PLLA)-poly(ethylene glycol) (PEG) multiblock copolymers were synthesized by polyesterification reaction of dicarboxylated PLLA with PEG in the presence of dicyclohexylcarbodiimide and N-dimethylaminopyridine. Dicarboxylated PLLA was prepared by a direct condensation polymerization of l-lactic acid with predetermined amounts of succinic acid, which was used to provide PLLA with a carboxylated terminal group. DSC and X-ray diffractometry of the multiblock copolymer suggested that PLLA and PEG blocks were phase separated and the crystallization behavior of one block was markedly affected by the presence of the other block, and in particular by the block length of the other block. The longer the PLLA block, the lower the crystallinity and the melting temperature of the PEG block. Multiblock copolymers crystallized from the melt and those from the solution casting showed different crystallization behavior, even though the chemical structures and the molecular weights were the same. The crystallizability of the PLLA block was more affected by the crystallization method than that of the PEG block." @default.
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• W2022883235 date "1999-12-01" @default.
• W2022883235 modified "2023-10-18" @default.
• W2022883235 title "Crystallization behavior of poly(l-lactide)-poly(ethylene glycol) multiblock copolymers" @default.
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• W2022883235 doi "https://doi.org/10.1016/s0014-3057(99)00024-5" @default.
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