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- W2022930078 abstract "Mg–Al layered double hydroxides (LDHs) were intercalated with various molecular-weight poly(oxypropylene)-bis-amidoacid salts (POP-acid), synthesized from polyoxyalkylene-diamines and maleic anhydride. The intercalation involves an ionic exchange reaction of LDHs at 120 °C and under N2 atmosphere in an autoclave to afford a series of organoclays with a maximal basal spacing of 92 Å, revealed by X-ray diffraction and transmission electron microscopy analyses. The unusually wide interlayer spacing was ascribed to the self-alignment of the hydrophobic POP backbone in the layer confinement. In contrast, the intercalation of poly(oxyethylene)-bis-amidoacids (POE-acid) afforded a low basal spacing (7.8 Å) due to their oxyethylene-backbone interaction with the layered surface. The resultant POP- and POE-acid intercalated LDHs also exhibited different dispersing properties in toluene or water. Particularly, the organically-modified and space-enlarged hybrids with a proper amount of the embedded POPs possessed an amphiphilic property of lowering the toluene/water interfacial tension." @default.
- W2022930078 created "2016-06-24" @default.
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- W2022930078 date "2004-10-01" @default.
- W2022930078 modified "2023-10-12" @default.
- W2022930078 title "Intercalation of layered double hydroxides by poly(oxyalkylene)-amidocarboxylates: tailoring layered basal spacing" @default.
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- W2022930078 doi "https://doi.org/10.1016/j.polymer.2004.09.031" @default.
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