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- W2022951606 abstract "The initial reaction in this three-step procedure for the radiochemical synthesis of L-[guanidinooxy-14C]canavanine involved the formation of barium [14C]cyanamide by reacting Ba14CO3 with ammonia at 950 degrees C. Barium [14C]cyanamide was converted to radioactive O-methylisourea, a guanidinating agent. L-[guanidinooxy-14C]Canavanine was formed by the reaction between the copper salt of L-canaline and [14C]O-methylisourea under alkaline conditions. The labeled canavanine was racemically pure as determined by enzyme-mediated hydrolysis. Reverse-phase HPLC and a novel colorimetric assay for cyanamide were used to quantify the reaction products. An overall yield for L-[guanidinooxy-14C]canavanine of approximately 25% was obtained." @default.
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- W2022951606 date "1983-09-01" @default.
- W2022951606 modified "2023-09-27" @default.
- W2022951606 title "Radiochemical synthesis of l-[guanidinooxy-14C]canavanine" @default.
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- W2022951606 doi "https://doi.org/10.1016/0003-2697(83)90083-0" @default.
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