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- W2022982059 abstract "A micro combustion calorimeter, internal bomb volume 4.5 cm3, has been built and tested. The calorimeter, intended for sample sizes around 10 mg, can be calibrated electrically as well as by combustion of benzoic acid. The standard deviation of the mean of a series of five experiments on 10 mg samples is ordinarily less than 0.02 per cent. The ratio of the energy equivalents, derived from benzoic acid and electrical calibrations, is 1.00019 with an uncertainty of ±0.00034 at a 95 per cent confidence level. The energy of combustion of 1,8-dimethylnaphthalene has been determined and is in good agreement with a recent macro determination. An ampoule technique for 5 to 8 mg solid samples with vapour pressures below approximately 20 Torr has been developed. The calorimeter fits the LKB 8700 precision calorimetry system." @default.
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- W2022982059 date "1973-09-01" @default.
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- W2022982059 title "A 4.5 cm3 bomb combustion calorimeter and an ampoule technique for 5 to 10 mg samples with vapour pressures below approximately 3 kPa (20 Torr)" @default.
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