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- W2023109853 abstract "The association of an effusion cell to a Tian-Calvet microcalorimeter offers the possibility of measuring, at 298.15 K, energies of vaporisation (or sublimation) of compounds, the vapour pressures of which range from 10−4 to 100 torr, with a reproducibility of 1%. The following results are obtained for enthalpies of vaporisation [(ΔHvap)m] of water (vapour pressure, 23.7 torr at 298.15 K), 43.84±0.29 kJ.mol−1; cyclohexane (vapour pressure, 97.5 torr at 298.15 K), 32.89±0.29 kJ.mol−1; hexamethylphosphotriamide (vapour pressure, 51.10−3 torr at 298.15 K), 61.1± 1.7 kJ.mol−1. In the present work, a critical study of the technique is also made. L'association d'une cellule d'effusion à un microcalorimètre Tian-Calvet a permis de mesurer à 1% près l'énergie mise en jeu lors de la sublimation ou de la vaporisation de composés dont la tension de vapeur est comprise entre 10−4 et 100 torr. Le présent travail expérimental a fourni, à 298,15 K, les enthalpies de vaporisation [(ΔHvap)m] de l'eau (43,84±0,29 kJ.mol−1), du cyclohexane (32,89±0,29 kJ.mol−1 et de l'hexaméthylphosphotriamide (61,1±1,7 kJ.mol−1) et a permis de faire une étude critique de la technique." @default.
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- W2023109853 date "1972-12-01" @default.
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- W2023109853 title "Mesures calorimétriques des enthalpies de vaporisation et de sublimation par effusion; mise au point de la technique" @default.
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- W2023109853 doi "https://doi.org/10.1016/0040-6031(72)85016-0" @default.
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