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- W2023118018 abstract "Phases of the Si-Al-O-N system are very important in the ceramic field. The reduction and simultaneous nitriding of aluminosilicate compounds permits the formation of alumina and sialons phases. Products of these reactions depend on several variables such as temperature, reaction time, metallic Al content, etc. In this work, reactions of Al with andalusite (Al2O3·SiO2) in N2 atmosphere were studied up to 1923 K. The crystalline phases formed were followed as a function of temperature, Al content and reaction time. Nitride phases were measured quantitatively using X-ray diffraction. Mullite and X-phase were formed during the reaction but the final products were mainly β′-sialon and α-Al2O3, The aluminium acts as a reducing agent and silicon appears at low temperatures. The reaction mechanism was established by taking the consideration of intermediate compounds, such as mullite and X-phase. Volatilization of SiO(g) took place during the reaction and was determined by weight loss and electron probe microanalysis." @default.
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- W2023118018 date "1997-03-01" @default.
- W2023118018 modified "2023-10-07" @default.
- W2023118018 title "Phase evolution of andalusite (Al2O3-SiO2)-Al system in nitrogen atmosphere" @default.
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- W2023118018 doi "https://doi.org/10.1016/s0254-0584(97)80074-0" @default.
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