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- W2023143036 abstract "Abstract The first total syntheses of oresbiusin A in the ( + )‐, ( – )‐, and (±)‐forms were accomplished in five steps with overall yields of ca. 70 %. The key intermediates with optical activity were generated through a Sharpless asymmetric dihydroxylation reaction. These efforts allowed us to establish the absolute configuration of this natural product with dextrorotary and a 2 S configuration. In addition, the total syntheses of both enantiomers of oresbiusin B along with its racemate were accomplished in six steps with overall yields of 58 %. Among these compounds, the unnatural oresbiusin A with a levorotary rotation was found to possess dose dependent anti‐HIV‐1 activity in H9 cells, whereas the other compounds were inactive." @default.
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- W2023143036 date "2012-07-26" @default.
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- W2023143036 title "First Total Syntheses of Oresbiusins A and B, Their Antipodes, and Racemates: Configuration Revision and Anti-HIV Activity" @default.
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- W2023143036 doi "https://doi.org/10.1002/ejoc.201200689" @default.
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