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- W2023174639 abstract "The 5,11- and 5,17-diisocyano-25,26,27,28-tetra-n-propoxycalix[4]arene bridging ligands (calix(NC) 2 ) have been prepared in four steps with 34 and 30% global yields, respectively. Their corresponding Ag(I) complexes have been prepared from the direct reaction of the ligand with AgBF 4 and are characterized from various spectroscopic and physical techniques. The MALDI-TOF spectra indicate the presence of polymers or oligomers of the type {Ag(calix(NC) 2 )(BF 4 )} n . The compounds have been characterized further from TGA, DSC, and XRD and compared with the oligomeric species 5,11,17,23-tetraisocyano-25,26,27,28-tetra-n-propoxycalix[4]arene silver(I) (as a BF 4 salt).Key words: silver, calix[4]arene, polymer, isocyanide, photosensitive, thermal gravimetric analysis." @default.
- W2023174639 created "2016-06-24" @default.
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- W2023174639 date "2003-11-01" @default.
- W2023174639 modified "2023-09-27" @default.
- W2023174639 title "Wide-rim functionalization of calix[4]arene: The di- and tetraisocyanocalix[4]arene assembling ligands and their silver(I) polymers and oligomers" @default.
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- W2023174639 doi "https://doi.org/10.1139/v03-116" @default.
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