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- W2023175849 abstract "Abstract The synthesis of the (±)‐form of the marine sesquiterpene (–)‐Δ 9(12) ‐capnellene ( 1 ) by double application of the a ‐alkynone cyclization is described. Starting with 2, 2, 5‐trim ethylcyclopentanone ( 2 ), the elaboration of the tricyclo [6.3.0.0 2,6 ]undecane C‐skeleton of 1 proceeded through the a ‐alkynone 3 , which was cyclized thermally to the bicyclo [3.3.0]octenone 4. For the anellation of the third five‐membered ring, 4 was transformed into the a ‐alkynone 5 and the latter cyclized thermally to a mixture of the angular triquinenone 6 and the linear triquinenone 7. The last steps in the synthesis of (±)‐Δ 9(12) ‐capnellene ( 1 ) were then accomplished from 7 by known methods." @default.
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- W2023175849 date "1982-12-15" @default.
- W2023175849 modified "2023-10-18" @default.
- W2023175849 title "Consecutive Application of the α‐Alkynone Cyclization: Total Synthesis of (±)‐Δ<sup>9(12)</sup>‐Capnellene" @default.
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- W2023175849 doi "https://doi.org/10.1002/hlca.19820650806" @default.
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