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• W2023185152 abstract "Die Kristallstrukturen der Titelverbindungen wurden röntgenographisch ermittelt. SeCl3+SbCl6−: Raumgruppe P21/m, Z = 4, Strukturlösung mit 1795 beobachteten unabhängigen Reflexen, R = 0,022. Gitterkonstanten bei −80°C: a = 940,9; b = 1066,3; c = 1234,9 pm; β = 102,79°. Die Verbindung bildet Ionenpaare mit der Struktur eines flächenverknüpften Doppeloktaeders. SeBr3+GaBr4−: Raumgruppe Pc, Z = 2, Strukturlösung mit 1461 beobachteten unabhängigen Reflexen, R = 0,058, Gitterkonstanten bei −60°C: a = 660,1; b = 655,3; c = 1431,3 pm; α = 101,17°. Die Verbindung kristallisiert im SCl3[AlCl4]-Strukturtyp. Zwischen den Ionen bestehen zwei relativ kurze Se … BrGa-Kontakte. PCl4+SeCl5−: Raumgruppe Ima2, Z = 8, Strukturlösung mit 1757 beobachteten unabhängigen Reflexen, R = 0,029. Gitterkonstanten bei −50°C; a = 1651,6; b = 1201,2; c = 1166,4 pm. Die SeCl5− -Ionen sind über interionische SeCl … Se-Kontakte entlang der kristallographischen c-Achse zu Ketten assoziiert. (PPh4+)2SeCl42− · 2CH3CN: Raumgruppe P21/n, Z = 2, Strukturlösung mit 2578 beobachteten unabhängigen Reflexen, R = 0,050. Gitterkonstanten bei −80°C: a = 1288,5; b = 726,0; c = 2585,8 pm; β = 101,65°. Die Verbindung enthält planar-quadratische SeCl42−-Ionen, die nahezu D4h-Symmetrie erfüllen. Crystal Structures of SeCl3+SbCl6−, SeBr3+GaBr4−, PCl4+SeCl5−, and (PPh4+)2SeCl42− · 2 CH3CN The crystal structures of the title compounds were determined by X-ray diffraction. SeCl3+SbCl6−: Space group P21/m, Z = 4, structure determination with 1795 observed unique reflections, R = 0.022. Lattice dimensions at −80°C: a = 940.9, b = 1066.3, c = 1234.9 pm, β = 102.79°. The compound forms ion pairs with the structure of a double octahedron with linked surfaces. SeBr3+GaBr4−: Space group Pc, Z = 2, structure determination with 1461 observed unique reflections, R = 0.058. Lattice dimensions at −60°C: a = 660.1, b = 655.3, c = 1431.3 pm, β = 101.177°. The compound crystallizes in the SCl3[AlCl4] lattice type. Between the ions there are two relatively short Se … BrGa contacts. PCl4+SeCl5−: Space group Ima2, Z = 8, structure determination with 1757 observed unique reflections, R = 0.029. Lattice dimensions at −50°C: a = 1651.6, b = 1201.2, c = 1166.4 pm. The SeCl5− ions are associated to chains via interionic SeCl … Se contacts along the crystallographic c-axis. (PPh4+)2SeCl42− · 2CH3CN: Space group P21/n, Z = 2, structure determination with 2578 observed unique reflections, R = 0.050. Lattice dimensions at −80°C: a = 1288.5, b = 726.0, c = 2585.8 pm, β = 101.65°. The compound includes planar-tetragonal SeCl42− ions, which almost meet D4h symmetry." @default.
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• W2023185152 title "Die Kristallstrukturen von SeCl3+SbCl6?, SeBr3+GaBr4?, PCl4+SeCl5? und (PPh4+)2SeCl42? � 2 CH3CN" @default.
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• W2023185152 doi "https://doi.org/10.1002/zaac.19966221108" @default.
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