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- W2023202468 abstract "Differential scanning calorimetry, (DSC) and inverse gas chromatography, (IGC) were used to analyze the miscibility and interactions in the poly(4-hydroxystyrene)/poly(vinyl methyl ether) (P4HS/PVME) system. The miscibility was assessed by the measurement of a single glass transition temperature, Tg, for each blend composition. The Tg—composition curve was analyzed in terms of Fox, Gordon—Taylor and Kovacs theories. The influence of molecular weight of P4HS in the presence of a cusp in the Tg—composition curve was discussed by comparison with previous Tg data. The IGC retention behaviour of the homopolymers and three blends (0.25,0.5 and 0.75 P4HS volume fractions) was realized at 190°C using selected probes. The polymer—polymer interaction parameters χ23 calculated from the Scott—Flory—Huggins formalism showed an apparent dependence on the probes. This dependence was analyzed using Horta's method based on the equation-of-state theory and a more simplified method proposed by Desphande. Negative values of χ23 confirmed the miscibility of the system. A blend composition dependence of χ23 was found, mainly determined by differences in the molecular surface-to-volume ratio of the polymers." @default.
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- W2023202468 date "1998-01-01" @default.
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- W2023202468 title "Miscibility and interactions in poly (vinyl methyl ether)/poly(4-hydroxystyrene) blends" @default.
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- W2023202468 doi "https://doi.org/10.1016/s0032-3861(97)00445-x" @default.
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