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- W2023203285 endingPage "4122" @default.
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- W2023203285 abstract "Reactions of a tripodal ligand, N,N′,N″-tris(3-pyridinyl)phosphoric triamide (TPPA), and a series of transition-metal ions result in the assembly of five discrete M6L8 coordination cages [M6(TPPA)8(H2O)12](ClO4)12·57H2O [M = Ni2+ (1), Co2+ (2), Zn2+ (3), Cd2+ (4)] and [Pd6(TPPA)8]Cl12·22H2O (5). X-ray structural analyses reveal that the cages have large internal cavities and flexible windows. The flexible ligand TPPA adopts the syn conformation in cages 1–4, but it transforms to the anti conformation in cage 5. Because of the conformational transformation, the sizes of the windows and the volume of the internal cavity of cage 5 are increased. 1H NMR and electrospray mass spectrometric studies show that cage 5 maintains its structural integrity in solution. Additionally, compounds 3 and 4 exhibit strong blue fluorescent emissions, which are 1 order of magnitude higher than that of the free ligand." @default.
- W2023203285 created "2016-06-24" @default.
- W2023203285 creator A5026733759 @default.
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- W2023203285 date "2012-03-22" @default.
- W2023203285 modified "2023-09-27" @default.
- W2023203285 title "Self-Assembly of Discrete M<sub>6</sub>L<sub>8</sub> Coordination Cages Based on a Conformationally Flexible Tripodal Phosphoric Triamide Ligand" @default.
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- W2023203285 doi "https://doi.org/10.1021/ic202373a" @default.
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