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• W202320402 endingPage "2660" @default.
• W202320402 startingPage "2654" @default.
• W202320402 abstract "A comparative study of the reactivity of dinitrogen acids [closo-1-CB9H8-1-COOH-10-N2] (3[10]) and [closo-1-CB9H8-1-COOH-6-N2] (3[6]) was conducted by diazotization of a mixture of amino acids [closo-1-CB9H8-1-COOH-6-NH3] (1[6]) and [closo-1-CB9H8-1-COOH-10-NH3] (1[10]) with NO+BF4− in the presence of a heterocyclic base (pyridine, 4-methoxypyridine, 2-picoline, or quinoline). The 10-amino acid 1[10] formed an isolable stable 10-dinitrogen acid 3[10], while the 6-dinitrogen carboxylate 3[6]− reacted in situ, giving products of N-substitution at the B6 position with the heterocyclic solvent (4[6]). The molecular and crystal structures for pyridinium acid 4[6]a were determined by X-ray crystallography. The electronic structures and reactivity of the 6-dinitrogen derivatives of the {1-CB9} cluster were assessed computationally at the B3LYP/6-31G(d,p) and MP2/6-31G(d,p) levels of theory and compared to those of the 10-dinitrogen, 2-dinitrogen, and 1-dinitrogen analogues." @default.
• W202320402 created "2016-06-24" @default.
• W202320402 creator A5024758586 @default.
• W202320402 creator A5029006414 @default.
• W202320402 creator A5057027437 @default.
• W202320402 date "2011-02-22" @default.
• W202320402 modified "2023-09-25" @default.
• W202320402 title "Diazotization of the Amino Acid [<i>closo</i>-1-CB₉H₈-1-COOH-6-NH₃] and Reactivity of the [<i>closo</i>-1-CB₉H₈-1-COO-6-N₂]⁻ Anion" @default.
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• W202320402 doi "https://doi.org/10.1021/ic102557s" @default.
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