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- W2023223995 abstract "Abstract High-resolution solid-state 13C NMR spectra of histidine powder samples prepared from solutions at several pH values near the pKa of the imidazole group are presented. These spectra demonstrate several effects due to the titration of the imidazole group. The chemical shifts for all of the carbon sites change upon titration. They are in “slow exchange” in the solid state in contrast to the “fast exchange” behavior seen in solution. Changes in the quadrupole interactions in the 14N sites occur upon titration and are observed by their effects on the resonance lineshapes of the 13C sites to which they are bonded." @default.
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- W2023223995 date "1986-01-01" @default.
- W2023223995 modified "2023-09-26" @default.
- W2023223995 title "The Effect of pH on solid-state 13C NMR spectra of histidine" @default.
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- W2023223995 doi "https://doi.org/10.1016/0022-2364(86)90112-5" @default.
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