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• W2023247625 endingPage "02BD07" @default.
• W2023247625 startingPage "02BD07" @default.
• W2023247625 abstract "The preparation of NiAl intermetallic compound nanoparticles was carried out by pulsed wire discharge (PWD) using twisted pure Ni and Al wires in N 2 ambient gas with varying number of turns of the wire ( N t ), energy ratio ( K ), and ambient gas pressure ( P ). From the voltage and current waveforms during the wire heating, the energy deposition ratio up to the voltage peak ( K p ) was calculated. It increased with an increase in N t to 0.4 turns/mm and with increases in K and P . Under all the conditions, with an increase in K p , the Ni composition ratio of the prepared particles ( C Ni ) became closer to that of the wire (= 51.2 mol %). Furthermore, the collection rate ( R c ) increased and the median particle diameter ( d 50 ) decreased. In particular, the change in d 50 due to the change in N t was not predicted by the relationship of d 50 and D th in our previous report. Single-phase NiAl intermetallic compound nanoparticles were successfully prepared under the condition in which N t is 0.4 turns/mm, K is 3.4, and P is 100 kPa, where relatively high value of K p was obtained. From these results, K p was determined to be an important factor that determines the composition, collection rate, and median diameter of intermetallic compound nanoparticles synthesized by PWD using different kinds of twisted wires under various experimental conditions. This may be because of the selective wire heating in high-resistance parts that are associated with the introduction of lattice defects and/or necks by overwinding." @default.
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• W2023247625 date "2014-01-29" @default.
• W2023247625 modified "2023-10-02" @default.
• W2023247625 title "Determining factor of median diameter in intermetallic compound nanoparticles prepared by pulsed wire discharge" @default.
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• W2023247625 doi "https://doi.org/10.7567/jjap.53.02bd07" @default.
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