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- W2023248380 abstract "A surfactant-assisted nonaqueous strategy, relying on high-temperature aminolysis of titanium carboxylate complexes, has been developed to access anisotropically shaped TiO2 nanocrystals selectively trapped in the metastable brookite phase. Judicious temporal manipulation of precursor supply to the reaction mixture enables systematic tuning of the nanostructure geometric features over an exceptionally wide dimensional range (30−200 nm). Such degree of control is rationalized within the frame of a self-regulated phase-changing seed-catalyzed mechanism, in which homogeneous nucleation, on one side, and heterogeneous nucleation/growth processes, on the other side, are properly balanced while switching from the anatase to the brookite structures, respectively, in a continuous unidirectional crystal development regime. The time variation of the chemical potential for the monomer species in the solution, the size dependence of thermodynamic structural stability of the involved titania polymorphs, and the reduced activation barrier for brookite nucleation onto initially formed anatase seeds play decisive roles in the crystal-phase- and shape-tailored growth of titania nanostructures by the present approach." @default.
- W2023248380 created "2016-06-24" @default.
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- W2023248380 date "2008-07-23" @default.
- W2023248380 modified "2023-10-01" @default.
- W2023248380 title "Nonhydrolytic Synthesis of High-Quality Anisotropically Shaped Brookite TiO<sub>2</sub> Nanocrystals" @default.
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- W2023248380 doi "https://doi.org/10.1021/ja803559b" @default.
- W2023248380 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/18646847" @default.
- W2023248380 hasPublicationYear "2008" @default.
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