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- W2023249596 abstract "Abstract Stage-n FeCl3-GICs (n = 2,3) prepared in the standard two-zone method were oxidized galvanostatically in H2SO4. The electrode potential vs. electric quantity curves observed during the treatment and the X-ray powder patterns of the products showed clearly the intercalation of H2SO4 into FeQ3-GICs and the formation of the graphite bi-intercalation compounds (GBCs) of FeCl3 and H2SO4. The c axis repeat distance Ic of the GBCs, 17.38A, from the stage-2 FeCl3-GIC was equal to the sum of those of FeCl3-GIC, 9.38A, and of H2SO4-GIC, 8.00A. From the stage-3 FeCl3-GIC the compound with Ic of 25.38A ( = 9.38A + 8.00A + 8.00A), through the intermediate with Ic of 20.73A ( = 9.38A + 3.35A + 8.00A). The electrochemical reduction of these GBCs suggested that the intercalation of H2SO4 into FeCl3-GICs is reversible." @default.
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- W2023249596 date "1990-01-01" @default.
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- W2023249596 title "Electrochemical preparation of the graphite bi-intercalation compound with H2SO4 and FeCl3" @default.
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- W2023249596 doi "https://doi.org/10.1016/0008-6223(90)90102-5" @default.
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