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- W2023264502 abstract "In order to experimentally ascertain the detection power afforded by the hollow cathode discharge (HCD) source in emission spectroscopy, various types of samples (solution dry residues, pelletted powders, electrically conducting materials) are analysed adopting in each case those working conditions which permit the signal-to-background ratio to be optimized. In all instances argon at a pressure of a few hundred Pa and current intensities not exceeding 400 mA are used. Spectra are recorded on films and evaluated microdensitometrically. The effects of the specimen's physical state as well as of the simultaneous presence of the other analytes are also elucidated. Detection limits are reported for Ag, Al, As, Bi, Cd, Cr, Cu, Fe, Ga, Mn, Ni, Pb, Se, Sn, Te, Ti and Zn. Experimental data support the view that the said effects are almost negligible. Only in the case of pelletted powders detection limits tend to worsen, this being probably due to the smaller surface subjected to discharge. The possibility of further improving the detection limits of HCD is finally outlined." @default.
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- W2023264502 date "1984-01-01" @default.
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- W2023264502 title "An investigation of the power of detection of the hollow cathode source in emission spectroscopy" @default.
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