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- W2023272951 abstract "The morphology of blends of polystyrene (PS) microgels with linear PS were studied using NMR spectroscopy. Three techniques were employed to assess the intimacy of mixing: isothermal cross-polarization/magic-angle-spinning (CP/MAS) dipolar dephasing 13C NMR, temperature-dependent 13C CP/MAS NMR, and one-pulse 1H MAS NMR. The experimental data reveal that linear PS can penetrate the core of soft microgels, whose network strands are substantially larger than the linear chains. However, when the microgel is highly cross-linked, such penetration is prevented. These results are in accord with Flory−Huggins swelling theory. Blends of linear PS with highly cross-linked microgels yield thermodynamically stable morphologies, in which the components are molecularly dispersed, yet segmental contacts are virtually absent. Such a phase morphology is novel and cannot be obtained with conventional polymer blends." @default.
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- W2023272951 date "2000-10-01" @default.
- W2023272951 modified "2023-09-24" @default.
- W2023272951 title "NMR Study of the Morphology of Polystyrene Linear/Microgel Blends" @default.
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- W2023272951 doi "https://doi.org/10.1021/ma000951x" @default.
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