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• W2023273668 abstract "The surface of supported tungstophosphoric acid H3PW12O40 (HPW) on all-silica MCM-41 has been investigated using high-resolution X-ray photoelectron spectroscopy (XPS) and X-ray absorption near edge structure (XANES). The results show the interaction between HPW and MCM-41 upon impregnation. Nuclear magnetic resonance (NMR) spectroscopy results also seem to confirm the above conclusion. Heating the supported acid increased the structural damage of HPW and MCM-41. Our results also suggest the formation of tungsten oxides on the surface upon heat treatment at 400 °C. A detailed analysis of the infrared (IR) spectra showed a gradual increase in the absorbance of the WOW corner shared vibration relative to the absorbance of the other bands. This indicates that the symmetry, and hence the stability of the bulk molecules were also decreased upon heating." @default.
• W2023273668 created "2016-06-24" @default.
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• W2023273668 date "2004-01-10" @default.
• W2023273668 modified "2023-09-24" @default.
• W2023273668 title "Surface investigation on thermal stability of tungstophosphoric acid supported on MCM-41 using synchrotron radiation" @default.
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• W2023273668 doi "https://doi.org/10.1016/j.apcata.2003.02.001" @default.
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