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- W2023275430 endingPage "2203" @default.
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- W2023275430 abstract "Abstract Methyl methacrylate (MMA) polymerizations have been conducted in the presence of large excesses of N ‐ tert ‐butyl‐ N ‐[1‐diethylphosphono‐(2,2‐dimethylpropyl) nitroxide] (SG1) at 110°C. It is demonstrated that such a protocol does not improve control/livingness in the nitroxide mediated polymerization (NMP) of this monomer, instead substantial levels of disproportionation between the nitroxide and propagating radical (PMMA • ) results. The extent of the disproportionation reaction increased with the SG1 concentration, eventually becoming the sole end forming event. Significant disproportionation between SG1 and PMMA • was also observed at substantially lower temperatures (45°C) in the presence of large excesses of SG1. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 2194–2203, 2007" @default.
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- W2023275430 date "2007-04-13" @default.
- W2023275430 modified "2023-10-17" @default.
- W2023275430 title "The role of excess nitroxide in the SG1 (N-tert-butyl-N-[1-diethylphosphono-(2,2-dimethylpropyl)] nitroxide)-mediated polymerization of methyl methacrylate" @default.
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- W2023275430 doi "https://doi.org/10.1002/pola.21986" @default.
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