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- W2023279537 abstract "Mesoporous silica containing isolated Ti with variable Si/Ti ratios was prepared by pyrolysis of a mixture of tetrakis(tris-tert-butoxysiloxy)titanium (TS4) and tetraethoxysilane (TEOS) through a hard template method. TEOS plays two roles as a silica source and solvent. TS4 works as a catalyst for the hydrolysis of TEOS. Titanium species are found to be isolated in the silica frameworks, supported by DR-UV-vis, FT-IR, ESR, and XPS. The mesoporous structure was verified by XRD, N2 adsorption, and SEM. The results of the catalytic performance for the oxidation reaction of cyclohexene using tert-butoxy hydrogen peroxide (TBHP) as oxidant show that high conversion (29%) of cyclohexene and selectivity (98%) of cyclohexene oxide are realized for the Ti-containing mesoporous silica with Si/Ti ratios of 28 and 51." @default.
- W2023279537 created "2016-06-24" @default.
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- W2023279537 date "2013-01-01" @default.
- W2023279537 modified "2023-09-24" @default.
- W2023279537 title "A novel route for preparation of Ti-containing mesoporous silica with high catalytic performance by using a molecular precursor tetrakis(tris-tert-butoxysiloxy)titanium" @default.
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- W2023279537 doi "https://doi.org/10.1039/c2ta01369j" @default.
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