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- W2023305083 abstract "The reaction of O-menthyl phenylphosphonite 1 with aromatic aldehydes in the presence of Me3SiCl provided the O-menthyl α-hydroxyphosphinates 2. Acidic hydrolysis of 2 gave the corresponding α-hydroxyphosphinic acids 3. The (+)-enantiomer of 3a and 3b, adduct of benzaldehyde and 4-methylbenzaldehyde respectively, were obtained via multiple recrystallization. The absolute configuration of (+)-3a was determined as S by X-ray crystallography. © 2003 Wiley Periodicals, Inc. Heteroatom Chem 14:312–315, 2003; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.10150" @default.
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- W2023305083 date "2003-01-01" @default.
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- W2023305083 title "Convenient synthesis of optically active ?-hydroxyphosphinic acids" @default.
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