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• W2023307931 abstract "Headspace solid-phase microextraction has been applied to the analysis of aroma compounds in vinegar. Silica fibre coated with Carboxen-polydimethylsiloxane was found to be more efficient at extracting these compounds than other fibres such as those coated with polydimethylsiloxane, Carbowax-divinylbenzene, and polydimethylsiloxane-divinylbenzene, but its repeatability was low. Different parameters such as extraction time, temperature of the sample during the extraction, ionic strength, and sample volume were optimised using a two-level factorial design expanded further to a central composite design. This chemometric tool is very appropriate in screening experiments where the aim is to investigate several possibly influential and/or interacting factors. The extraction efficiency is inversely affected by the acetic acid content-an increase in the acetic acid concentration decreases the extraction efficiency. No interference is observed with the increase in content of polyphenols." @default.
• W2023307931 created "2016-06-24" @default.
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• W2023307931 date "2002-04-01" @default.
• W2023307931 modified "2023-09-27" @default.
• W2023307931 title "Optimisation of headspace solid-phase microextraction for analysis of aromatic compounds in vinegar" @default.
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• W2023307931 doi "https://doi.org/10.1016/s0021-9673(02)00122-x" @default.
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