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- W2023335197 abstract "Uranium isotope ratios can provide source information for tracking uranium contamination in a variety of fields, ranging from occupational bioassay to monitoring aftereffects of nuclear accidents. We describe the development of isotope selective laser ionization spectrometry for ultratrace measurement of the minor isotopes 234U, 235U, and 236U with respect to 238U. The inherent isotopic selectivity of three-step excitation with single-mode continuous wave lasers results in measurement of the minor isotopes at relative abundances below 1 ppm and is not limited by isobaric interferences such as 235UH+ during measurement of 236U. This relative abundance limit is attained without mass spectrometric analysis of the laser-created ions. Uranyl nitrate standards from an international blind comparison were used to test analytical performance for different isotopic compositions and with quantities ranging from 11 ng to 10 μg total uranium. Isotopic ratio determination was demonstrated over a linear dynamic range of 7 orders of magnitude with a few percent relative precision and detection limits below 500 fg for the minor isotopes." @default.
- W2023335197 created "2016-06-24" @default.
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- W2023335197 date "2008-07-09" @default.
- W2023335197 modified "2023-10-14" @default.
- W2023335197 title "Ultratrace Uranium Fingerprinting with Isotope Selective Laser Ionization Spectrometry" @default.
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- W2023335197 doi "https://doi.org/10.1021/ac800764j" @default.
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