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- W2023349916 abstract "The chemical shifts of all the ring protons of the three Man residues in a pentaantennary glycan chain have been unambiguously assigned by two-dimensional proton nuclear magnetic resonance (1H-NMR) spectroscopic methods. The study, using chemical shift and J values on the conformation of the trimannosyl unit, revealed that the rotamer about the C5-C6 bond of the alpha 1-->6 linkage in the sequence of Man alpha 1-->6Man beta 1--> is predominantly confined to a gauche-gauche rotamer (omega = 180 degrees, omega = O6-C6-C5-H5) and not to a gauche-trans rotamer (omega = -60 degrees). We do not know of any previous demonstration that the dihedral angle omega (O6-C6-C5-H5) in Man alpha 1-->6Man beta 1--> is preferentially 180 degrees in complex-type N-linked glycans having no bisecting GlcNAc residue." @default.
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- W2023349916 date "1995-03-01" @default.
- W2023349916 modified "2023-10-13" @default.
- W2023349916 title "Proton NMR Study of the Trimannosyl Unit in a Pentaantennary N-Linked Decasaccharide Structure. Complete Assignment of the Proton Resonances and Conformational Characterization" @default.
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- W2023349916 doi "https://doi.org/10.1111/j.1432-1033.1995.tb20328.x" @default.
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