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- W2023356940 abstract "Abstract Living cationic polymerization of 2‐adamantyl vinyl ether (2‐vinyloxytricyclo[3.3.1.1] 3,7 decane; 2‐AdVE) was achieved with the CH 3 CH(OiBu)OCOCH 3 /ethylaluminum sesquichloride/ethyl acetate [CH 3 CH(OiBu)OCOCH 3 /Et 1. 5 AlCl 1. 5 /CH 3 COOEt] initiating system in toluene at 0 °C. The number‐average molecular weights ( M n 's) of the obtained poly(2‐AdVE)s increased in direct proportion to monomer conversion and produced the polymers with narrow molecular weight distributions (MWDs) ( M w / M n = ∼1.1). When a second monomer feed was added to the almost polymerized reaction mixture, the added monomer was completely consumed and the M n 's of the polymers showed a direct increase against conversion of the added monomer. Block and statistical copolymerization of 2‐AdVE with n ‐butyl vinyl ether (CH 2 CHOCH 2 CH 2 CH 2 CH 3 ; NBVE) were possible via living process based on the same initiating system to give the corresponding copolymers with narrow MWDs. Grass transition temperature ( T g ) and thermal decomposition temperature ( T d ) of the poly(2‐AdVE) (e.g., M n = 22,000, M w / M n = 1.17) were 178 and 323 °C, respectively. © 2008 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 46: 1629–1637, 2008" @default.
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- W2023356940 date "2008-01-22" @default.
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- W2023356940 title "Living cationic polymerization of 2-adamantyl vinyl ether" @default.
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- W2023356940 doi "https://doi.org/10.1002/pola.22502" @default.
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