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- W2023372598 abstract "The crystal and molecular structures of the two bis(amine) complexes of rhenium(I), [ReBr(CO)3(NHR2)2](R = Me or Et), have been studied by X-ray diffraction methods. The complexes crystallize in the monoclinic system, space group P21/n, with cell constants (R = Me)a= 9.023(3), b= 11.537(4), c= 12.199(4)A, β= 97.28(3)°; and (R = Et)a= 7.340(2), b= 9.784(3), c= 22.742(6)A, β= 95.05(2)°. The molecular structure in both cases consists of facially arranged ligands around six-co-ordinate rhenium(I); the two cis amine ligands do not interact appreciably either by intra- or inter-molecular hydrogen bonding. The ethyl derivative reacts with CO2 to give the corresponding carbamato-complex [Re(CO)3(O2CNEt2)(NHEt2)], the latter showing association in solution presumably due to intermolecular hydrogen bonding." @default.
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- W2023372598 date "1981-01-01" @default.
- W2023372598 modified "2023-09-25" @default.
- W2023372598 title "Preparation, properties, and crystal and molecular structures of bis(dialkylamine) complexes of rhenium(I)" @default.
- W2023372598 doi "https://doi.org/10.1039/dt9810002523" @default.
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