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- W2023378182 abstract "C39H41ClFeNO2PPd, monoclinic, P121/n1 (no. 14), a = 9.971(2) A, b = 23.823(5) A, c = 17.396(4) A, = 100.15(3)°, V = 4067.8 A 3 , Z =4 ,Rgt(F) = 0.074, wRref(F 2 ) = 0.209, T = 293 K. Source of material To a stirred solution of [(N-methyl-N-p-methoxybenzyl)amino]ethylferrocene (182 mg, 0.5 mmol) and sodium acetate (41 mg, 0.5 mmol) in methanol (20 ml) was added dropwise a solution of sodium tetrachloropalladate(II) (150 mg, 0.5 mmol) in methanol (15 ml). The mixture was stirred at room temperature for one hour. Triphenylphosphine (220 mg, 0.8 mmol) was then added and the resulted mixture was stirred for another 30 min. Solvent was removed in vacuo and the residue was recrystallized from anhydrous diethyl ether/petroleum ether (30 - 60 °C) to afford the target final product in the yield of 50 %. Crystals were grown by slow evaporation of an ethyl acetate/petroleum ether solution (60 -9 0 °C) (v/v = 3:1) at room temperature over a period of one month." @default.
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- W2023378182 date "2008-09-01" @default.
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- W2023378182 title "Crystal structure of chloro(2-{1-[N-methyl-N-(4-methoxybenzyl)- amino]ethyl}ferrocenyl-k2N,C1)(triphenylphosphine-kP)palladium(II) monohydrate, [FePd(C5H5)(C16H19NO)Cl(PPh3)] · H2O" @default.
- W2023378182 doi "https://doi.org/10.1524/ncrs.2008.0102" @default.
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