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- W2023381880 abstract "Octadecyl-silylated silicas (ODSs) end-capped by high-temperature silylation (HTS) with various organic silicon agents have been characterized by high-performance liquid chromatography of pyridine and diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy. All the agents exhibit end-capping effects, except for trimethylchlorosilane, and bifunctional agents being the most effective. Some of the ODSs end-capped by HTS show OH bands at 3700 and 3670 cm−1 on DRIFT spectra, and others show an OH band only at 3670 cm−1. The ODSs without the OH band at 3700 cm−1 have lower adsorptivity for pyridine. The OH band area in DRIFT spectra shows a good correlation with the separation factor (α) of phenol against pyridine." @default.
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- W2023381880 date "1997-01-01" @default.
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- W2023381880 title "Optimization of end-capping of octadecyl-silylated silica gels by high-temperature silylation" @default.
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- W2023381880 doi "https://doi.org/10.1016/s0021-9673(96)00679-6" @default.
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