Matches in SemOpenAlex for { <https://semopenalex.org/work/W2023409950> ?p ?o ?g. }
Showing items 1 to 92 of
92
with 100 items per page.
- W2023409950 endingPage "1622" @default.
- W2023409950 startingPage "1616" @default.
- W2023409950 abstract "A simple, rapid and sensitive ultra performance liquid chromatography tandem mass spectrometry method was developed and fully validated for the quantitative determination of seven amphetamines and metabolites in urine. The method was validated for selectivity, linearity, LOQ, LOD, imprecision, bias, analyte and processed sample stability, matrix effect, recovery, carryover and dilution integrity. A classic liquid–liquid extraction with ethyl acetate was used as sample preparation procedure. The compounds were separated on an Acquity UPLC HSS C18 column in 6.8 min. The linear dynamic range was established from 25 to 500 ng/mL. The limit of quantification was fixed to the lowest calibrator level and the limit of detection ranged from 0.125 to 2.5 ng/mL. The method presented an excellent intra- and inter-assay imprecision and bias (<10.7%) at each measured concentration of two external quality controls (QC) and three “in house” QC. No matrix effects were observed and good recoveries (>70%) were obtained for all the compounds. No carryover was observed after the analysis of high concentrated samples (8000 ng/mL). The method was subsequently applied to authentic samples." @default.
- W2023409950 created "2016-06-24" @default.
- W2023409950 creator A5006536172 @default.
- W2023409950 creator A5019109448 @default.
- W2023409950 creator A5019638914 @default.
- W2023409950 creator A5027767150 @default.
- W2023409950 creator A5044766996 @default.
- W2023409950 date "2010-06-01" @default.
- W2023409950 modified "2023-10-16" @default.
- W2023409950 title "Analysis of amphetamines and metabolites in urine with ultra performance liquid chromatography tandem mass spectrometry" @default.
- W2023409950 cites W1526055455 @default.
- W2023409950 cites W1967595833 @default.
- W2023409950 cites W1990112228 @default.
- W2023409950 cites W1992073724 @default.
- W2023409950 cites W2001574197 @default.
- W2023409950 cites W2001843221 @default.
- W2023409950 cites W2008201261 @default.
- W2023409950 cites W2016968987 @default.
- W2023409950 cites W2026073861 @default.
- W2023409950 cites W2030353836 @default.
- W2023409950 cites W2047997746 @default.
- W2023409950 cites W2089032617 @default.
- W2023409950 cites W2097113529 @default.
- W2023409950 cites W2126259752 @default.
- W2023409950 cites W2164036543 @default.
- W2023409950 cites W97951617 @default.
- W2023409950 doi "https://doi.org/10.1016/j.jchromb.2010.03.048" @default.
- W2023409950 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20413354" @default.
- W2023409950 hasPublicationYear "2010" @default.
- W2023409950 type Work @default.
- W2023409950 sameAs 2023409950 @default.
- W2023409950 citedByCount "24" @default.
- W2023409950 countsByYear W20234099502012 @default.
- W2023409950 countsByYear W20234099502013 @default.
- W2023409950 countsByYear W20234099502014 @default.
- W2023409950 countsByYear W20234099502015 @default.
- W2023409950 countsByYear W20234099502016 @default.
- W2023409950 countsByYear W20234099502017 @default.
- W2023409950 countsByYear W20234099502021 @default.
- W2023409950 countsByYear W20234099502022 @default.
- W2023409950 crossrefType "journal-article" @default.
- W2023409950 hasAuthorship W2023409950A5006536172 @default.
- W2023409950 hasAuthorship W2023409950A5019109448 @default.
- W2023409950 hasAuthorship W2023409950A5019638914 @default.
- W2023409950 hasAuthorship W2023409950A5027767150 @default.
- W2023409950 hasAuthorship W2023409950A5044766996 @default.
- W2023409950 hasConcept C10390740 @default.
- W2023409950 hasConcept C106487976 @default.
- W2023409950 hasConcept C119128265 @default.
- W2023409950 hasConcept C162356407 @default.
- W2023409950 hasConcept C179998833 @default.
- W2023409950 hasConcept C185592680 @default.
- W2023409950 hasConcept C2778576202 @default.
- W2023409950 hasConcept C31827203 @default.
- W2023409950 hasConcept C43617362 @default.
- W2023409950 hasConcept C4725764 @default.
- W2023409950 hasConcept C64489805 @default.
- W2023409950 hasConcept C95986675 @default.
- W2023409950 hasConceptScore W2023409950C10390740 @default.
- W2023409950 hasConceptScore W2023409950C106487976 @default.
- W2023409950 hasConceptScore W2023409950C119128265 @default.
- W2023409950 hasConceptScore W2023409950C162356407 @default.
- W2023409950 hasConceptScore W2023409950C179998833 @default.
- W2023409950 hasConceptScore W2023409950C185592680 @default.
- W2023409950 hasConceptScore W2023409950C2778576202 @default.
- W2023409950 hasConceptScore W2023409950C31827203 @default.
- W2023409950 hasConceptScore W2023409950C43617362 @default.
- W2023409950 hasConceptScore W2023409950C4725764 @default.
- W2023409950 hasConceptScore W2023409950C64489805 @default.
- W2023409950 hasConceptScore W2023409950C95986675 @default.
- W2023409950 hasIssue "19" @default.
- W2023409950 hasLocation W20234099501 @default.
- W2023409950 hasLocation W20234099502 @default.
- W2023409950 hasOpenAccess W2023409950 @default.
- W2023409950 hasPrimaryLocation W20234099501 @default.
- W2023409950 hasRelatedWork W1973892552 @default.
- W2023409950 hasRelatedWork W1987886540 @default.
- W2023409950 hasRelatedWork W2005997170 @default.
- W2023409950 hasRelatedWork W2008161654 @default.
- W2023409950 hasRelatedWork W2044145238 @default.
- W2023409950 hasRelatedWork W2050801935 @default.
- W2023409950 hasRelatedWork W2087917523 @default.
- W2023409950 hasRelatedWork W2117645760 @default.
- W2023409950 hasRelatedWork W2141316828 @default.
- W2023409950 hasRelatedWork W2552274597 @default.
- W2023409950 hasVolume "878" @default.
- W2023409950 isParatext "false" @default.
- W2023409950 isRetracted "false" @default.
- W2023409950 magId "2023409950" @default.
- W2023409950 workType "article" @default.