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• W2023442986 abstract "Titanium phosphate, Na3[Ti2P2O10F]·xH2O (1), has been synthesized under hydrothermal conditions and structurally characterized using powder X-ray diffraction, neutron diffraction, and selected area electron diffraction (SAED). 1 crystallizes in the tetragonal space group I4/mmm with a = 6.4207(1) Å and c = 10.6762(2) Å and can be described by the stacking of a square-net sheet consisting of alternative linkage of TiFO5 octahedra and PO4 tetrahedra. The TiFO5 octahedron is highly distorted, with a short “titanyl” Ti−O bond and a long Ti−F bond. The “titanyl” oxygen is almost doubly bonded to Ti; the square-net sheets are linked only by sharing common F atoms, which lead to a rather opened framework containing 2D channels in the ab plane. The counter cations Na+ and water molecules reside in the channels. At high temperature, the adsorbed water molecules escape from the channels, leading to an anhydrous phase Na3[Ti2P2O10F] (2) with exactly the same structural framework as that of 1. 2 is stable at high temperature in an Ar atmosphere, but decomposes to other known titanium phosphates and oxide at about 650 °C in air. The Na ions in the compound are exchangeable. In addition, 2 exhibits a Na conductivity comparable to that of the NASICON type titanium phosphates (1.0 × 10-4 Ω-1 cm-1 at 200 °C)." @default.
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• W2023442986 date "2007-01-24" @default.
• W2023442986 modified "2023-09-27" @default.
• W2023442986 title "Na₃[Ti₂P₂O₁₀F]: A New Oxyfluorinated Titanium Phosphate with an Ionic Conductive Property" @default.
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• W2023442986 doi "https://doi.org/10.1021/cm062513w" @default.
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