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- W2023459452 abstract "Abstract In this paper, we reported a method to prepare monodisperse magnetite nanoparticles at mild temperature using cheap and non-toxic precursors. It overcomes the shortages of chemical co-precipitation method and thermal decomposition method and combines the advantages of facile, cheap, large-scale, monodisperse, nanosize, and low synthesis temperature and low toxic. In this method, FeCl 3 · 6H 2 O, FeCl 2 · 4H 2 O and sodium oleate were mixed in toluene/ethanol/water mixture solvent and refluxed at 74 °C to prepare magnetite nanoparticles directly. The nanoparticles were characterized by transmission electron microscopy, dynamic light scattering, X-ray diffraction, X-ray photoelectron spectroscopy, Fourier transform infrared spectrometer and thermogravimetric analysis. The magnetic properties of nanoparticles were measured by superconducting quantum interference device. The results showed that the nanoparticles are well-monodisperse with about 4–5 nm of average diameter. The nanoparticles were proved to be superparamagnetic with saturated magnetization 23.6 emu/g and blocking temperature 24.4 K. A possible formation mechanism of monodisperse magnetite nanoparticles was presented at the same time." @default.
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- W2023459452 date "2008-08-01" @default.
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- W2023459452 title "Preparation of monodisperse magnetite nanoparticles under mild conditions" @default.
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- W2023459452 doi "https://doi.org/10.1016/j.cap.2007.09.003" @default.
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