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- W2023479950 abstract "Abstract The growth behavior of self-assembled monolayer (SAM) films formed from Cl 3 SiC 11 H 22 OCOCH 3 (C 11 Ac) and Cl 3 SiC 16 H 32 SCOCH 3 (C 16 Sc) on oxidized Si wafers at room temperature was investigated using atomic force microscopy (AFM), water contact angle measurements, and ellipsometry. Both silanes form thin films via nucleation of islands, similar to the growth behavior of n -octadecyltrichlorosilane (OTS) SAMs, although the island morphology is distinct for each molecule. Near-confluent monolayer films are obtained for both C 11 Ac and C 16 Sc after substrate immersion periods of 10–60 min. The ellipsometric thickness of both types of SAMs is less than that expected for a close-packed, all- trans ensemble of methylene chains aligned parallel to the substrate surface normal, suggesting a liquid crystalline-like structure in which methylene groups are present at the outer film surface. This model is supported by surface wettability data obtained on C 11 Ac SAMs that were reduced in situ to generate hydroxy-terminated films. When the deposition time is greater than 1 h, C 11 Ac forms highly disordered films of multilayer thickness that are much rougher than the films obtained at shorter deposition times. Multilayer formation is not observed with C 16 Sc, although increased deposition times also result in adsorption of additional, submonolayer amounts of material." @default.
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- W2023479950 date "1999-12-01" @default.
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- W2023479950 title "Growth behavior and structure of alkyltrichlorosilane monolayers bearing thioacetate and acetate tailgroups" @default.
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- W2023479950 doi "https://doi.org/10.1016/s0928-4931(99)00138-1" @default.
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