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• W2023481289 abstract "The shape-controlled synthesis of nanoparticles was established in single-phase solutions by controlling growth directions of crystalline facets on seed nanocrystals kinetically; however, it was difficult to rationally predict and design nanoparticle shapes. Here we introduce a methodology to fabricate nanoparticles in smaller sizes by evolving shapes thermodynamically. This strategy enables a more rational approach to fabricate shaped nanoparticles by etching specific positions of atoms on facets of seed nanocrystals in reverse micelle reactors where the surface energy gradient induces desorption of atoms on specific locations on the seed surfaces. From seeds of 12-nm palladium nanocubes, the shape is evolved to concave nanocubes and finally hollow nanocages in the size ~10 nm by etching the centre of {200} facets. The high surface area-to-volume ratio and the exposure of a large number of palladium atoms on ledge and kink sites of hollow nanocages are advantageous to enhance catalytic activity and recyclability." @default.
• W2023481289 created "2016-06-24" @default.
• W2023481289 creator A5022358427 @default.
• W2023481289 creator A5045867002 @default.
• W2023481289 date "2014-05-14" @default.
• W2023481289 modified "2023-10-17" @default.
• W2023481289 title "Rational strategy for shaped nanomaterial synthesis in reverse micelle reactors" @default.
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• W2023481289 doi "https://doi.org/10.1038/ncomms4870" @default.
• W2023481289 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4112590" @default.
• W2023481289 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/24828960" @default.
• W2023481289 hasPublicationYear "2014" @default.
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