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• W2023484458 abstract "The reaction system MnCl2/2Na2S2/2.2CS2/Et4NSH/2Et4NCl in acetonitrile affords (Et4N)3[Mn(CS4)2Cl] in high yield. Upon prolonged standing, (Et4N)2[Mn(S6)2] was isolated from the reaction mixture filtrate. The structures of these compounds were determined by X-ray crystallography. [Mn(CS4)2Cl]3− exhibits a distorted square pyramidal stereochemistry with chloride in the apical position and two five-membered chelate rings formed by the infrequently encountered perthiocarbonate ligand. Indistinguisable C—S bond distances to coordinated and free sulphur atoms at a common carbon atom indicate ligand delocalization. In [Mn(S6)2]2− the manganese atom occurs in an irregular tetrahedral coordination formed by two chelating hexasulphido ligands. This work adds to the small group of sulphur-rich manganese complexes of established structures." @default.
• W2023484458 created "2016-06-24" @default.
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• W2023484458 date "1993-01-01" @default.
• W2023484458 modified "2023-10-17" @default.
• W2023484458 title "Tetrahedral and square-pyramidal sulphur-rich complexes of manganese(II)" @default.
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• W2023484458 doi "https://doi.org/10.1016/s0277-5387(00)81637-x" @default.
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