FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2023485911> ?p ?o ?g. }

• W2023485911 endingPage "784" @default.
• W2023485911 startingPage "775" @default.
• W2023485911 abstract "A herb-combined prescription, mainly derived from roots of Salvia miltiorrhiza and Panax notoginseng, has been widely used for improving coronary or cerebral circulation in China as well as in Western countries. Multiple commercially available preparations, known as Fufang Danshen preparations (FDPs), produced by various manufacturers with the raw materials from different sources, pose a serious challenge to the quality control of this herb medicine. Previous pharmacological studies identify three types of bioactive components correlated with the clinical effect of those herb preparations. Those mainly include four phenolic acids, four saponins and four diterpenoid quinones. In this report, by using high performance liquid chromatography (HPLC) coupled with diode array and evaporative light scattering detectors (DAD-ELSD), we developed an improved quality control method for those herb medicines. A simultaneous separation and quantification of the 12 components was performed on a C(18) column, in which the mobile phase consisted of (A) 0.1% aqueous formic acid and (B) acetonitrile using a gradient elution. The optimum detection wavelength was set at 281 nm, the drift tube temperature of ELSD was set at 113 degrees C, the nitrogen flow rate at 3.1L/min, and the gain=4. All calibration curves showed good linear regression (r(2)>0.9927) within test ranges. The method developed showed good precision and accuracy with overall intra- and inter-day variations of 0.64-4.79% and 0.69-4.96%, respectively, and the overall recoveries of 93.50-107.69% for the 12 compounds analyzed. This method was successfully applied to quantify the twelve components in ten commercial samples from three formulas by seven independent manufacturers. This readily available, low-cost and reliable HPLC-DAD-ELSD method improved the quality control of traditional Chinese medicinal preparations consisting of complex compounds with different structures such as FDPs." @default.
• W2023485911 created "2016-06-24" @default.
• W2023485911 creator A5008637608 @default.
• W2023485911 creator A5025530383 @default.
• W2023485911 creator A5030189609 @default.
• W2023485911 creator A5043418591 @default.
• W2023485911 creator A5051866342 @default.
• W2023485911 creator A5076761099 @default.
• W2023485911 date "2007-12-01" @default.
• W2023485911 modified "2023-10-03" @default.
• W2023485911 title "Improved quality control method for Fufang Danshen preparations through simultaneous determination of phenolic acids, saponins and diterpenoid quinones by HPLC coupled with diode array and evaporative light scattering detectors" @default.
• W2023485911 cites W1982430126 @default.
• W2023485911 cites W1995805103 @default.
• W2023485911 cites W2005349276 @default.
• W2023485911 cites W2005397161 @default.
• W2023485911 cites W2012840245 @default.
• W2023485911 cites W2020400577 @default.
• W2023485911 cites W2020632156 @default.
• W2023485911 cites W2033471462 @default.
• W2023485911 cites W2034635074 @default.
• W2023485911 cites W2059288684 @default.
• W2023485911 cites W2064657996 @default.
• W2023485911 cites W2071759898 @default.
• W2023485911 cites W2073620735 @default.
• W2023485911 cites W2073809331 @default.
• W2023485911 cites W2075020423 @default.
• W2023485911 cites W2075467088 @default.
• W2023485911 cites W2078040953 @default.
• W2023485911 cites W2079598269 @default.
• W2023485911 cites W2085426077 @default.
• W2023485911 cites W2093049883 @default.
• W2023485911 cites W2145903836 @default.
• W2023485911 cites W2154066769 @default.
• W2023485911 doi "https://doi.org/10.1016/j.jpba.2007.07.013" @default.
• W2023485911 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17720349" @default.
• W2023485911 hasPublicationYear "2007" @default.
• W2023485911 type Work @default.
• W2023485911 sameAs 2023485911 @default.
• W2023485911 citedByCount "70" @default.
• W2023485911 countsByYear W20234859112012 @default.
• W2023485911 countsByYear W20234859112013 @default.
• W2023485911 countsByYear W20234859112014 @default.
• W2023485911 countsByYear W20234859112015 @default.
• W2023485911 countsByYear W20234859112016 @default.
• W2023485911 countsByYear W20234859112017 @default.
• W2023485911 countsByYear W20234859112018 @default.
• W2023485911 countsByYear W20234859112021 @default.
• W2023485911 countsByYear W20234859112023 @default.
• W2023485911 crossrefType "journal-article" @default.
• W2023485911 hasAuthorship W2023485911A5008637608 @default.
• W2023485911 hasAuthorship W2023485911A5025530383 @default.
• W2023485911 hasAuthorship W2023485911A5030189609 @default.
• W2023485911 hasAuthorship W2023485911A5043418591 @default.
• W2023485911 hasAuthorship W2023485911A5051866342 @default.
• W2023485911 hasAuthorship W2023485911A5076761099 @default.
• W2023485911 hasConcept C110084920 @default.
• W2023485911 hasConcept C142724271 @default.
• W2023485911 hasConcept C179998833 @default.
• W2023485911 hasConcept C185592680 @default.
• W2023485911 hasConcept C188947578 @default.
• W2023485911 hasConcept C204787440 @default.
• W2023485911 hasConcept C2776332195 @default.
• W2023485911 hasConcept C2777379063 @default.
• W2023485911 hasConcept C2779091547 @default.
• W2023485911 hasConcept C2779824472 @default.
• W2023485911 hasConcept C2991655182 @default.
• W2023485911 hasConcept C43617362 @default.
• W2023485911 hasConcept C556039675 @default.
• W2023485911 hasConcept C59822182 @default.
• W2023485911 hasConcept C71924100 @default.
• W2023485911 hasConcept C86803240 @default.
• W2023485911 hasConceptScore W2023485911C110084920 @default.
• W2023485911 hasConceptScore W2023485911C142724271 @default.
• W2023485911 hasConceptScore W2023485911C179998833 @default.
• W2023485911 hasConceptScore W2023485911C185592680 @default.
• W2023485911 hasConceptScore W2023485911C188947578 @default.
• W2023485911 hasConceptScore W2023485911C204787440 @default.
• W2023485911 hasConceptScore W2023485911C2776332195 @default.
• W2023485911 hasConceptScore W2023485911C2777379063 @default.
• W2023485911 hasConceptScore W2023485911C2779091547 @default.
• W2023485911 hasConceptScore W2023485911C2779824472 @default.
• W2023485911 hasConceptScore W2023485911C2991655182 @default.
• W2023485911 hasConceptScore W2023485911C43617362 @default.
• W2023485911 hasConceptScore W2023485911C556039675 @default.
• W2023485911 hasConceptScore W2023485911C59822182 @default.
• W2023485911 hasConceptScore W2023485911C71924100 @default.
• W2023485911 hasConceptScore W2023485911C86803240 @default.
• W2023485911 hasIssue "5" @default.
• W2023485911 hasLocation W20234859111 @default.
• W2023485911 hasLocation W20234859112 @default.
• W2023485911 hasOpenAccess W2023485911 @default.
• W2023485911 hasPrimaryLocation W20234859111 @default.
• W2023485911 hasRelatedWork W2066601363 @default.
• W2023485911 hasRelatedWork W2094650009 @default.
• W2023485911 hasRelatedWork W2095444318 @default.
• W2023485911 hasRelatedWork W2324538553 @default.
• W2023485911 hasRelatedWork W2353733990 @default.
• W2023485911 hasRelatedWork W2355921991 @default.

• next